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THREE METAL-ORGANIC POLYMERS ASSEMBLED FROM Cd(ll)-FLLCONAZOLE: SYNTHESES, CRYSTAL STRUCTURES, AND CHARACTERIZATION

Three new complexes [Cd(Hflu):(N03)](N03) 1, [Cd(H20)(Hflu)2(Hmalo)](N03)-2(H20) 2, and [Cd(H20)(Htlu):(Hrum)](N05)-2(H:0) 3 (Hflu = [2-(2,4-difluorophenyl)-l,3-bis( 1,2,4-triazol-l-yl)-propan-2-ol]. H:fum = fumaric acid, H:malo = malonate acid) are synthesized by a solution diffusion method and characterized by single crystal X-ray diffraction methods, elemental analyses. IR spectroscopy as well as thermal analyses. In compound 1, Cd(II) cations are bridged by fluconazole ligands to form 2D Cd—Hflu layers, and these layers are further connected by С—H---F hydrogen bonds to form a complicated 3D structure with the topology of (4-6-8)(4-64-84-10)(6-3). Compounds 2 and 3 arc isostructural, and in them the Cd(II) cations are bridged by fluconazole ligands to form a 2D network, which is connected by С—H -О hydrogen bonds to form a complicated 3D (3,4)-conncctcd framework with the topology of (4-82)(4-85).

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H:fum = fumaric acid, H:malo = malonate acid) are synthesized by a solution diffusion method and characterized by single crystal X-ray diffraction methods, elemental analyses. <...> IR spectroscopy as well as thermal analyses. <...> In compound 1, Cd(II) cations are bridged by fluconazole ligands to form 2D Cd—Hflu layers, and these layers are further connected by С—H---F hydrogen bonds to form a complicated 3D structure with the topology of (4-6-8)(4-64-84-10)(6-3). <...> Compounds 2 and 3 arc isostructural, and in them the Cd(II) cations are bridged by fluconazole ligands to form a 2D network, which is connected by С—H -О hydrogen bonds to form a complicated 3D (3,4)-conncctcd framework with the topology of (4-82)(4-85).! <...> H:fum = fumaric acid, H:malo = malonate acid) are synthesized by a solution diffusion method and characterized by single crystal X-ray diffraction methods, elemental analyses. <...> IR spectroscopy as well as thermal analyses. <...> In compound 1, Cd(II) cations are bridged by fluconazole ligands to form 2D Cd—Hflu layers, and these layers are further connected by С—H---F hydrogen bonds to form a complicated 3D structure with the topology of (4-6-8)(4-64-84-10)(6-3). <...> Compounds 2 and 3 arc isostructural, and in them the Cd(II) cations are bridged by fluconazole ligands to form a 2D network, which is connected by С—H -О hydrogen bonds to form a complicated 3D (3,4)-conncctcd framework with the topology of (4-82)(4-85).! <...>
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